CUED Publications database

Microstructural evolution in infiltration-growth processed MgB₂ bulk superconductors

Bhagurkar, AG and Yamamoto, A and Dennis, A and Durrell, JH and Aljohani, TA and Nadendla, HB and Cardwell, DA (2017) Microstructural evolution in infiltration-growth processed MgB₂ bulk superconductors. Journal of the American Ceramic Society, 100. pp. 2451-2460.

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The study reports phase and microstructural evolution in MgB2 bulk superconductors fabricated by an infiltration and growth (IG) process. Three distinct stages, (1) intermediate boride formation, (2) bulk liquid Mg infiltration, and (3) MgB2 layer formation, were identified in IG process after detailed examination of series of samples prepared with varied heating conditions. The intermediate phase Mg2B25, isomorphous to β-boron, was detected prior to MgB2 phase formation in stage (1). Due to volume expansion involved in stage 1, cracks formed in the β-boron particles and propagated radially inwards during stage 3. The growing MgB2 particles sintered simultaneously with formation of grain boundaries during the process, as evidenced by the measured hardness and critical current density in these samples. From our observations, we estimate the total time needed for complete transformation to MgB2.

Item Type: Article
Divisions: Div C > Materials Engineering
Depositing User: Unnamed user with email
Date Deposited: 17 Jul 2017 19:26
Last Modified: 09 Sep 2021 03:09
DOI: 10.1111/jace.14792